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Synthesis and Characterization of Pectin–Chitosan crosslinked of BADGE for Adsorbents Candidate of Textile Dye Waste Water

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@article{IJASEIT10655,
   author = {Budi Hastuti and Saptono Hadi and Warih Purwendah},
   title = {Synthesis and Characterization of Pectin–Chitosan crosslinked of BADGE for Adsorbents Candidate of Textile Dye Waste Water},
   journal = {International Journal on Advanced Science, Engineering and Information Technology},
   volume = {10},
   number = {1},
   year = {2020},
   pages = {351--355},
   keywords = {pectin; chitosan; Pec-Chi-BADGE; membrane; dye wastewater.},
   abstract = {

The increasing development of the textile industry in Indonesia has resulted in a negative effect on the dyes' wastewater that can pollute the environment. There are several methods developed to reduce the dyestuff levels in water pollution, such as coagulation and flocculation, membrane filtration, adsorption, precipitation, photocatalytic degradation, ion exchange, advanced oxidation, and biological treatment. In order to find out the solution, it is necessary to process liquid dyes waste, which has several advantages, including the relatively low cost and high efficiency in the process of absorbing liquid dyes. Commercial Chitosan and Pectin, Bisphenol A Diglysidyl Ether (BADGE) were purchased from Sigma Aldrich (Germany), Aceton, Acetic Acid 5%, and Aquadest. Mesoporous Pectin-Chitosan crosslinked BADGE (Pec-Chi-BADGE) membrane was successfully synthesized by the coacervation method, by mixing chitosan solution in 5% acetic acid and pectin solution in aqua dest, then added BADGE as a crosslinker to the solution.  The structure and surface characteristics of Chi-Pec-BADGE membranes were analysed using Fourier transform infra-red (FTIR) spectroscopy, scanning electron microscopy (SEM), and XRD. Based on the FTIR characterization indicate that pectin chitosan crosslinked BADGE was successfully synthesized. The results showed that Chi-Pec-BADGE membranes could show the shift of peaks characterized by FTIR meant interactions of functional groups carboxyl, amine, and hydrogen. The results of XRD show that the Chi-Pec-BADGE membranes characteristic was amorphous. Furthermore, SEM data shows that the structure of the adsorbent was porous.

},    issn = {2088-5334},    publisher = {INSIGHT - Indonesian Society for Knowledge and Human Development},    url = {http://ijaseit.insightsociety.org/index.php?option=com_content&view=article&id=9&Itemid=1&article_id=10655},    doi = {10.18517/ijaseit.10.1.10655} }

EndNote

%A Hastuti, Budi
%A Hadi, Saptono
%A Purwendah, Warih
%D 2020
%T Synthesis and Characterization of Pectin–Chitosan crosslinked of BADGE for Adsorbents Candidate of Textile Dye Waste Water
%B 2020
%9 pectin; chitosan; Pec-Chi-BADGE; membrane; dye wastewater.
%! Synthesis and Characterization of Pectin–Chitosan crosslinked of BADGE for Adsorbents Candidate of Textile Dye Waste Water
%K pectin; chitosan; Pec-Chi-BADGE; membrane; dye wastewater.
%X 

The increasing development of the textile industry in Indonesia has resulted in a negative effect on the dyes' wastewater that can pollute the environment. There are several methods developed to reduce the dyestuff levels in water pollution, such as coagulation and flocculation, membrane filtration, adsorption, precipitation, photocatalytic degradation, ion exchange, advanced oxidation, and biological treatment. In order to find out the solution, it is necessary to process liquid dyes waste, which has several advantages, including the relatively low cost and high efficiency in the process of absorbing liquid dyes. Commercial Chitosan and Pectin, Bisphenol A Diglysidyl Ether (BADGE) were purchased from Sigma Aldrich (Germany), Aceton, Acetic Acid 5%, and Aquadest. Mesoporous Pectin-Chitosan crosslinked BADGE (Pec-Chi-BADGE) membrane was successfully synthesized by the coacervation method, by mixing chitosan solution in 5% acetic acid and pectin solution in aqua dest, then added BADGE as a crosslinker to the solution.  The structure and surface characteristics of Chi-Pec-BADGE membranes were analysed using Fourier transform infra-red (FTIR) spectroscopy, scanning electron microscopy (SEM), and XRD. Based on the FTIR characterization indicate that pectin chitosan crosslinked BADGE was successfully synthesized. The results showed that Chi-Pec-BADGE membranes could show the shift of peaks characterized by FTIR meant interactions of functional groups carboxyl, amine, and hydrogen. The results of XRD show that the Chi-Pec-BADGE membranes characteristic was amorphous. Furthermore, SEM data shows that the structure of the adsorbent was porous.

%U http://ijaseit.insightsociety.org/index.php?option=com_content&view=article&id=9&Itemid=1&article_id=10655 %R doi:10.18517/ijaseit.10.1.10655 %J International Journal on Advanced Science, Engineering and Information Technology %V 10 %N 1 %@ 2088-5334

IEEE

Budi Hastuti,Saptono Hadi and Warih Purwendah,"Synthesis and Characterization of Pectin–Chitosan crosslinked of BADGE for Adsorbents Candidate of Textile Dye Waste Water," International Journal on Advanced Science, Engineering and Information Technology, vol. 10, no. 1, pp. 351-355, 2020. [Online]. Available: http://dx.doi.org/10.18517/ijaseit.10.1.10655.

RefMan/ProCite (RIS)

TY  - JOUR
AU  - Hastuti, Budi
AU  - Hadi, Saptono
AU  - Purwendah, Warih
PY  - 2020
TI  - Synthesis and Characterization of Pectin–Chitosan crosslinked of BADGE for Adsorbents Candidate of Textile Dye Waste Water
JF  - International Journal on Advanced Science, Engineering and Information Technology; Vol. 10 (2020) No. 1
Y2  - 2020
SP  - 351
EP  - 355
SN  - 2088-5334
PB  - INSIGHT - Indonesian Society for Knowledge and Human Development
KW  - pectin; chitosan; Pec-Chi-BADGE; membrane; dye wastewater.
N2  - 

The increasing development of the textile industry in Indonesia has resulted in a negative effect on the dyes' wastewater that can pollute the environment. There are several methods developed to reduce the dyestuff levels in water pollution, such as coagulation and flocculation, membrane filtration, adsorption, precipitation, photocatalytic degradation, ion exchange, advanced oxidation, and biological treatment. In order to find out the solution, it is necessary to process liquid dyes waste, which has several advantages, including the relatively low cost and high efficiency in the process of absorbing liquid dyes. Commercial Chitosan and Pectin, Bisphenol A Diglysidyl Ether (BADGE) were purchased from Sigma Aldrich (Germany), Aceton, Acetic Acid 5%, and Aquadest. Mesoporous Pectin-Chitosan crosslinked BADGE (Pec-Chi-BADGE) membrane was successfully synthesized by the coacervation method, by mixing chitosan solution in 5% acetic acid and pectin solution in aqua dest, then added BADGE as a crosslinker to the solution.  The structure and surface characteristics of Chi-Pec-BADGE membranes were analysed using Fourier transform infra-red (FTIR) spectroscopy, scanning electron microscopy (SEM), and XRD. Based on the FTIR characterization indicate that pectin chitosan crosslinked BADGE was successfully synthesized. The results showed that Chi-Pec-BADGE membranes could show the shift of peaks characterized by FTIR meant interactions of functional groups carboxyl, amine, and hydrogen. The results of XRD show that the Chi-Pec-BADGE membranes characteristic was amorphous. Furthermore, SEM data shows that the structure of the adsorbent was porous.

UR - http://ijaseit.insightsociety.org/index.php?option=com_content&view=article&id=9&Itemid=1&article_id=10655 DO - 10.18517/ijaseit.10.1.10655

RefWorks

RT Journal Article
ID 10655
A1 Hastuti, Budi
A1 Hadi, Saptono
A1 Purwendah, Warih
T1 Synthesis and Characterization of Pectin–Chitosan crosslinked of BADGE for Adsorbents Candidate of Textile Dye Waste Water
JF International Journal on Advanced Science, Engineering and Information Technology
VO 10
IS 1
YR 2020
SP 351
OP 355
SN 2088-5334
PB INSIGHT - Indonesian Society for Knowledge and Human Development
K1 pectin; chitosan; Pec-Chi-BADGE; membrane; dye wastewater.
AB 

The increasing development of the textile industry in Indonesia has resulted in a negative effect on the dyes' wastewater that can pollute the environment. There are several methods developed to reduce the dyestuff levels in water pollution, such as coagulation and flocculation, membrane filtration, adsorption, precipitation, photocatalytic degradation, ion exchange, advanced oxidation, and biological treatment. In order to find out the solution, it is necessary to process liquid dyes waste, which has several advantages, including the relatively low cost and high efficiency in the process of absorbing liquid dyes. Commercial Chitosan and Pectin, Bisphenol A Diglysidyl Ether (BADGE) were purchased from Sigma Aldrich (Germany), Aceton, Acetic Acid 5%, and Aquadest. Mesoporous Pectin-Chitosan crosslinked BADGE (Pec-Chi-BADGE) membrane was successfully synthesized by the coacervation method, by mixing chitosan solution in 5% acetic acid and pectin solution in aqua dest, then added BADGE as a crosslinker to the solution.  The structure and surface characteristics of Chi-Pec-BADGE membranes were analysed using Fourier transform infra-red (FTIR) spectroscopy, scanning electron microscopy (SEM), and XRD. Based on the FTIR characterization indicate that pectin chitosan crosslinked BADGE was successfully synthesized. The results showed that Chi-Pec-BADGE membranes could show the shift of peaks characterized by FTIR meant interactions of functional groups carboxyl, amine, and hydrogen. The results of XRD show that the Chi-Pec-BADGE membranes characteristic was amorphous. Furthermore, SEM data shows that the structure of the adsorbent was porous.

LK http://ijaseit.insightsociety.org/index.php?option=com_content&view=article&id=9&Itemid=1&article_id=10655 DO - 10.18517/ijaseit.10.1.10655