Two Uncoating Techniques for Measuring Cold-Formed Steel Residual Stress Using Cos-α X-ray Diffraction Method

Tri Widya Swastika (1), Heru Purnomo (2), Henki Wibowo Ashadi (3), Muhammad Refai Muslih (4), Rifky Apriansyah (5), Mohd Syahrul Hisyam bin Mohd Sani (6)
(1) Civil Engineering Department, Universitas Indonesia, Jl. Lingkar, Depok, Indonesia
(2) Civil Engineering Department, Universitas Indonesia, Jl. Lingkar, Depok, Indonesia
(3) Civil Engineering Department, Universitas Indonesia, Jl. Lingkar, Depok, Indonesia
(4) Neutron Scattering Lab. PRTDRAN-BRIN, Serpong, Indonesia
(5) Neutron Scattering Lab. PRTDRAN-BRIN, Serpong, Indonesia
(6) Civil Engineering Studies, Collage of Engineering, Universiti Teknologi MARA, Pahang, Malaysia
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Swastika, Tri Widya, et al. “Two Uncoating Techniques for Measuring Cold-Formed Steel Residual Stress Using Cos-α X-Ray Diffraction Method”. International Journal on Advanced Science, Engineering and Information Technology, vol. 14, no. 6, Dec. 2024, pp. 2008-17, doi:10.18517/ijaseit.14.6.20549.
The cold-bending effect during the roll-forming process may affect the material's mechanical properties and induce residual stress in the cold-formed steel sections. Cos-α X-ray Diffraction is an appropriate method for measuring residual stress in cold-formed steel due to the materials' thinness. This method also offers excellent precision and simplicity. However, the limited penetrating ability of X-rays, which extend only a few microns, significantly hinders the measurement of residual stresses in cold-formed steel when coatings are present. Therefore, this study will implement two uncoating or de-coating techniques for measuring residual stress using the cos-α X-ray Diffraction method on the surface of cold-formed steel with a 50 μm layer of aluminum-zinc coating. These techniques include water sanding and chemical solutions. Two procedures are performed for the chemical solution: the first procedure combines a 25% hydrochloric acid (HCl) solution with a 25% ammonium hydroxide (NH4OH) solution, while the second procedure uses only a 25% hydrochloric acid (HCl) solution. This study demonstrates that the second procedure effectively removes the surface coating from cold-formed steel and provides a good classification of cos-α X-ray Diffraction intensity data related to the Debye-Scherrer ring. A combination of 25% hydrochloric acid (HCl) and 25% ammonium hydroxide (NH4OH) solution results in a mediocre classification. On the other hand, the water sanding technique produced more bad classifications. Furthermore, the key to the success of the cos-α X-ray Diffraction method is removing the coating from the cold-formed steel.

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